doi:10.16597/j.cnki.issn.1002-154x.2022.03.010
从小试实验到中试放大———浅谈分子筛中试放大合成中的一些问题及思考
杜凯敏1,2 卓佐西1,2 胡晨晖1,2 祁志福1,2 刘春红1,2∗
(1. 浙江浙能技术研究院有限公司,浙江 杭州 311121; 2. 浙江省火力发电高效节能与污染物控制技术研究重点实验室,浙江 杭州 311121)
From Bench-Scale Test to Pilot-Scale Test-Discussion on some Problems and Thinking of Molecular Sieve Pilot-Scale Synthesis
Du Kaimin 1,2; Zhuo Zuoxi 1,2; Hu Chenhui 1,2; Qi Zhifu 1,2; Liu Chunhong 1,2∗;
(1. Zhejiang Energy R & D Institute Co. Ltd. , Zhejiang Hangzhou 311121; 2. Key Laboratory of Energy Conservation & Pollutant Control Technology for Thermal Power of Zhejiang Province, Zhejiang Hangzhou 311121)
摘要:
中试放大合成分子筛过程中,由于设备及操作方式等差异,都可能导致“放大效应”的产生致使合成失败。 本文从原料、反应器、投料、分离洗涤、干燥焙烧、三废等方面对分子筛合成从小试实验到中试放大中存在的差异问题进行了评述和思考。
关键词：小试实验；中试放大；分子筛合成；问题和思考；
Abstract：
The failure of synthesis may be caused by the amplification effect due to the difference of equipment and operation in the pilot-scale synthesis process. This paper reviews and considers the differences in the synthesis of molecular sieve from bench-scale test to pilot-scale test, such as raw materials, reactors, feeding, separation, washing, drying, roasting and wastes.
Keywords：sbench-scale test; pilot-scale test; molecular sieve synthesis; problems and thinking;